Ai SolventVap 5L Evaporator w/ Cold Trap Condenser & Power Lift

Save $197.60 USD

Price:
Sale price$4,742.40 USD Regular price$4,940.00 USD
Description

Ai SolventVap 5L series rotary evaporators is now ETL tested to UL/CSA standards. This certification is required by many municipalities, and it also provides a higher standard of equipment safety and lifespan. SolventVap come with all PTFE valves for solvent-resistant operations. Also come with them are vertical glassware and digital temperature/rotation control. Its optimized bath volume allows for rapid heat-up times. Thats why our SolventVap evaporators consistently deliver reliable and reproducible process results that are usually reserved for more costly systems. Another important aspect of the SolventVap is the safety features, which includes dry-run protection, water bath over-temperature shut-off protection, and fuse protection.

Rotary evaporator features a specially designed motor and worm gear, which provides constant rotation at speeds from 10 to 180 rpm. As the flask containing the solvent is rotated, it continually transfers a thin layer of liquid over the entire inner surface. This gives a very large surface area for evaporation, which is caused by the gentle heating from the water bath. The rotating system is fitted with a special seal that allows the apparatus to be placed under vacuum, effectively reducing the boiling point of the solvents and removing the vapor phase, making the process much more efficient. Each unit is also equipped with an easy-to-use vacuum release and a continuous feed system, which allows solvent to be constantly drawn into the rotating flask without needing to stop the operation.

Digital water bath operates from ambient temperature to 99C (210F) with PID temperature control stepping at 0.1C increments. Heating coils are located directly inside the pan for the most efficient heating possible. A built-in overheat protector will shut down power, should the controller fail.

Standard Glassware Set includes 1.32 gallon (5 liters) round-bottomed evaporating flask, 0.79 gallon (3 liters) round-bottomed receiving flask, and vertical cold trap condenser. Rotary evaporators with vertical condenser for are great for distillation of solvents with higher boiling points.

Features

  • ETL tested to UL and CSA standards. CE certification optional.
  • No chiller needed, utilizes dry ice for optimal efficiency.
  • Water bath cover gives you uniform temperature inside evaporation flask as well as energy saving by reducing heat loss. It also creates a better lab environment by preventing heat and humidity from escaping.
  • Solvent-resistant PTFE and Viton gaskets, ensuring long time operation.
  • Specialized motor with extremely compact, intermeshed worm and worm gear provides precise driving for very quiet, vibration-free operation.
  • Downward-condensing vacuum connection design ensures safe vacuum operation.
  • Motorized water bath lifting for precise control.
  • Easy, straight-forward visual operation with digital speed and temperature display.
  • PID temperature controller ensures accurate temperature control is maintained.
  • One year warranty on rotary evaporator except for glassware and all sealing gaskets.

Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

 

 

 

 


 

A rotary evaporator is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. The process of rotary evaporation is most often used to separate solvents with low boiling points, such a n-hexane or ethyl acetate, from compounds which are solid at room temperature and pressure. However, careful application also allows for the removal of a solvent from a sample containing a liquid compound, if there is minimal co-evaporation (azeotropic behavior) and a sufficient difference in boiling points at the chosen temperature and reduced pressure.

 

 

Example: The following table illustrates a variety of substances, ordered by increasing vapor pressure (in absolute units).

 

Rotary Evaporator Frequently Asked Questions

  1. Q: What type of plug is needed for my rotary evaporator?
    A: The type of plug will depend on the model of rotary evaporator and whether the unit is a 110V or 220V model. Please consult the table below for further details:

Rotary Evaporator Model

Voltage (V)

Plug Type

2L

110/220

Bath: 6-15P (220V)                                                                                                        Motor Housing: 5-15P (110V)

5L

110

L5-30P

220

6-20P

10L

110

not available

220

L6-30P

20L

110

not available

220

L6-30P

50L

110

not available

220

L6-30P

 

  1. Q: What is the temperature range of the rotary evaporator
    A: The temperature range of the rotary evaporator is 20-99C.

  2. Q: What is the maximum pressure that the glass condenser’s coil is rated to? What is the maximum pressure that the condenser itself is rated to?
    A: The glass condenser’s coil is rated to 14 psi and the condenser itself is only rated for atmospheric pressure and a vacuum of 3 torr.

 

  1. Q: What is the dual receiving flask kit used for on the 20 and 50L rotary evaporators?
    A: The dual receiving flask kit is used to remove reclaimed solvent from the evaporator without interrupting its operation.

  2. Q: What heating medium can be used in the water bath?
    A: Only distilled water can be used as a heating medium in the water bath of an Across International rotary evaporator.

  3. Q: Can the vacuum level be set on the rotary evaporator?
    A: The vacuum level can be set only when a vacuum controller is purchased with the rotary evaporator. Please speak to sales or check the rotary evaporator’s customization section on the website for recommendations.

 

  1. Q: What accessories come with the purchase of a rotary evaporator?
    A: The accessories that come with each model will be different depending on the unit purchased. An accessories list can be found on the unit’s website listing and can be found in the standard package tab.

  2. Q: What is the evaporation speed of my rotary evaporator?
    A: The evaporation speed of the rotary evaporator will depend on what is being evaporated, and the parameters chosen. Please refer to the table for the estimated evaporation rate for ethanol and water.

Rotary Evaporator Model

Solvent Evaporated

Evaporation Speed

2L

Ethanol

20mL/min

Water

5L

Ethanol

3.79 L/Hr

Water

1.89 L/Hr

10L

Ethanol

5.68 L/Hr

Water

2.84 L/Hr

20L

Ethanol

7.5 L/Hr

Water

3.78 L/Hr

50L

Ethanol

7.5 L/Hr

Water

15 L/Hr

 

 

  1. Do the rotary evaporator’s come UL listed, are there any exceptions.
    A: All Across International rotary evaporators are UL listed at no additional cost but must be specified as UL on the order.

  2. Does Across International offer a CE option for their line of rotary evaporators? Are there any additional costs associated with this option?
    A: Across International offers a TUV listening to CE standards for all rotary evaporators aside from the 2L, and the pricing schedule is shown below


 

2L

5L

10L

20L

50L

CE Certificaiton Price

N/A

$1,000

$2,000

$3,000

$3,000

 

 

 

ecifications
Electrical requirements
110V 60Hz single phase, 2300 watts, 21A
or
220V 50/60Hz single phase, 2300 watts, 10.5A
Rotation motor: 300 watts
Glass material High borosilicate glass 3.3
Evaporating flask
Capacity: 1.32 gallon (5 liters)
Maximum load: Not to exceed 60% of the flask's capacity
Sealing flange: 2" diameter
Rotation speed: 10 to 140 rpm
Evaporating speed: 0.5 gallon/hour (water), 1 gallon/hour (alcohol)
Receiving flask
0.79 gallon (3 liter)
Condenser Glassware: Vertical cold trap (dry ice) condenser with lid
Vacuum connection: 3/8" hose barb x 1
Working environment
5 to 95F
Water bath
Temperature range: ambient to 99C (210F)
Temperature controller: digital
Dimensions: 11.4" diameter x 6.7" depth x 9" height
Material: stainless steel
Media: distilled water only
Max. water level: not to exceed 1" from the top rim of the bath
Number of heaters: one
Drain port: one
Exterior liner: rubber
Lifting: motoriezed
Maximum lifting distance: 4 inches
Vacuum
Vacuum level: < 3 torrs
Sealing: PTFE + Viton gaskets
Connection: 3/8" hose barb x 1
Safety Dry-run, over-temp shut-off, built-in circuit breakers
Shipping weight 105 Lb (evaporator), 57 Lb (glassware)
Unit dimensions
30 x 15.7 x 42" (WxDxH)
Shipping dimensions 29 x 17 x 35" (evaporator), 22 x 22 x 22" (glassware) (WxDxH)
Compliance UL 61010-1: 2012 Ed.3 + R: 29 Apr 2016
CSA C22.2# 61010-1-12: 2012 Ed.3+ U1; U2 (R2017)
CE

 

Standard package

 

 Part description

 Quantity

Part image

 Ai SolventVap 1.3-gallon rotary evaporator and water bath
1 set

 Vertical cold trap condenser with 1 vacuum port and lid, glass

1 pc
 1.32G/5L round shaped rotating evaporating flask, glass
1 pc
 3L receiving flask with detachable drain port
1 pc
 Three-way tee vapor buffering flask, glass
1 pc
 Glass receiving flask & condenser connector elbow with PTFE open/close switch 1 set
 Receiving flask glass vacuum port with PTFE open/close valve
1 set
 Glass material feeding port with PTFE open/close valve
1 set  
 Glass vapor duct and PTFE vacuum seal kit (pre-installed)
1 pc
 PTFE extension feeding hose 1 pc
 Stainless steel pole and mechanical vacuum gauge with 2 hose barb connection
1 pc
 Rubber-wrapped condenser and receiving flask support and bracket 3 pcs
 Flask quick clamp (4 smaller pcs for condenser, receiving flask and feeder, 1 larger pc for 3-way flask) & centering ring
6 sets
 GL14 connector
1 pc
 Allen key and backup inner hex screws 4 pcs
 Ai plexiglass water bath cover for SolventVap 5L 1 pc
 Users manual 1 pc

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