Description
Ai R150 series jacketed glass reactors are designed for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Each reactor features adjustable stirring speeds and a constant pressure feeding funnel that allows you to add material to the vessel at a uniform and controlled speed. The built-in condenser makes it possible to recover some materials, also at a controlled rate of speed.
Features
- ETL certified to UL and CSA standards
- Includes a FREE high quality thermo insulation jacket (a $999 value) with open/close viewing window and top/bottom adjustable drawstrings, specially designed and made for Ai glass jacketed reactors. These jackets will extend chiller life, allow you to go down to a lower temperature, and also cut your utility bill.
- Solvent-resistant PTFE on all sealing components ensures long time durability and operation.
- Adjustable stirring rate provides great torque or high speed.
- Patented PTFE stirring rod bearing for reliable and quiet operation.
- Optional multi-layer stirring blades for optimal reaction results.
- Large condenser cooling surface for exceptional condensation performance.
- Rugged stainless steel reinforced PTFE stirrer with anchored agitator, suitable for a wide range of viscous materials.
- Easily visual operation with digital speed and temperature displays.
- Heavy duty stainless steel supporting framework with lockable casters for mobility and stability. (whole support and glass vessel shipped pre-assembled).
- Mobile and detachable 316L stainless steel splash bin available for an additional cost.
Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.
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PTFE/PVDF CIP Spray Ball
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FAQ for Glass Reactor Series
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When do you recommend using the different impeller types that you have listed on the website?
The two different impeller types that we have is the pitched blade and the anchor agitator. It is recommended to use the pitched impeller for low viscosity solutions such as aqueous solutions and organic solvents. The anchor impeller is best used for higher viscosity applications such as thick oils, resins, and polymers.
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How do I clean my reactor?
The most effective and efficient way to clean your reactor would be by using the clean in place kit shown below paired with a pump capable of achieving between 10-20 psi.
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What is the best way to fill the reactor?
The best way to fill the reactor is to pull vacuum on the reactor from the condenser, and use either the stopcock on the lid or other fitting connected to a hose to pull the suck fluid into the reactor. As long as the other end of the tube is submerged in liquid and the pressure inside of the reactor is less than atmospheric pressure, fluid will enter the reactor.
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What are the materials of construction for the reactorās wetted parts?
3 borosilicate glass and PTFE
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How long is the warranty period and what does it cover?
The length of the warranty is one year, and it covers manufacturing defects,
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What accessories come with the reactor?
The reactor will come with everything listed on the standard package for the unit that will be purchased. If purchasing an entire turnkey, please see the turnkeyās standard package. The standard package can be found on the web listing at Across Internationalās website under the standard package tab.
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Where can I find technical information about the Across International reactor?
Technical information can be found on the Across International website under the specifications tab. If further technical information is needed, please reach out to the sales team via email or phone at Across International: or 888-980899.
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What are the lid port sizes for my glass reactor?
The lid port sizes will vary depending on reactor type. Any port not labelled on the drawing is specific to Across International, take note that the QC-35 is also specific to Across International but clamps and adapters can be bought from Across International as needed for all lid adapters.
Lid for 10-50L reactorļ¼
Lid for 100L-200L reactor:
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Will these sizes fit standard American ground glass joints? If so which ones will fit?
Please see the table below for a detailed description of which Across International glass reactor joints will fit the standard American ground glass joints:
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Across International Joints Conical Joints |
Compatible American Standard Conical Joints |
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40/38 |
40/50 |
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34/35 |
34/45 |
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24/29 |
24/40 |
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14/23 |
14/35 |
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| Model | R150 |
| Electrical requirements |
110V 60Hz or 220V 50/60Hz, 1-Phase, 750W |
| Stirring motor | Power: 750 watts Speed: 300 rpm max. Torque: 14.7 N.m max. Protection: IP44 Speed ratio: 1:3 |
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Condenser surface area
|
0.8m^2 |
| Reaction glass vessel capacity |
40 gallons (150L) |
| Cooling/heating jacket capacity |
12 gallons (45L, Approx.) |
| Feeding flask capacity | 2.6 gallons (10L) |
| Condenser receiving flask capacity | 5.3 gallons (20L) |
| Ports on vessel lid | Stirrer: #60 flange x 1 Temp sensor: #35 flange x 1 Condenser: #50 ball joint x 1 Liquid feeding: #34 joint x 2 Solid feeding: #95 flange x 1 Feeding funnel port: #40 joint x 1 |
| Glass material | High borosilicate glass 3.3 |
| Maximum jacket pressure |
4.4 psi or 0.03 MPa |
| Drain valve | Flush seal design with large opening and flat flange clamp |
| Agitator | Style: impeller Material: 304 stainless steel with PTFE liner |
| Funnel | Pressure equalizing |
| Vacuum gauge | Mechanical |
| Swivel caster | Four |
| Glass vessel temperature range |
-110F to 400F |
| Vacuum level | Ā 20 torr |
| Vacuum sealing | Glass or PTFE |
| Mobile splash bin |
Material: 316L stainless steel Dimensions: 20.5 x 27 x 7" (WxDxH) |
| Drain port ground clearance |
17 inches |
| Unit/shipping dimesions (WxDxH) |
48 x 41 x 109" / 77 x 61 x 43" |
| Compliance | ETL listed to UL and CSA standards (optional), CE (optional) |
| Shipping weight | 650 Lbs / 870 Lbs |
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Ā Part description |
Ā Quantity |
Part image |
| Glass vessel, lid, clamps, and heavy-duty stainless-steel stand with casters (shipped pre-assembled) |
1 set |
|
| Ā Glass vessel insulation jacket with openable viewing window | 1 pc | Ā |
| Rubber bumper (pre-assembled) | 1 pc | |
| Lid Gaskets (pre-assembled) | 1 pc | |
| Upper and lower clamp set (pre-assembled) | 1 pc | |
|
Ā Vertical condenser with dual cooling coils, 2 chilling fluid ports, and 1 vacuum port, glass |
1 pc |
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| Ā Glass condenser dispenser with drain port and PTFE open/close valve |
1 set |
|
| Ā Glass feeding funnel with PTFE open/close valve |
1 set | |
| Ā Glass receiving flask with PTFE open/close valve | 1 set | |
| Ā 1" Glass bottom drain port with PTFE open/close valve |
1 set |
|
| Ā Glass vacuum valve (R-GVV34 x 2, R-GVV40 x 1, R- GVV24 x 3) |
6 sets | |
| Ā Stirring motor controller with material temperature display (Motor RPM and Material Temperature) | 1 set | Ā Ā |
| Ā Stirring motor and motor support w/shaft guard cover |
1 set | Ā |
| Ā USB Cable | 1 pc | |
| Ā Mechanical vacuum gauge with two 3/8" hose barb ports |
1 pc | |
| Ā Temperature probe with PTFE seal with #35 clamp |
1 pc | |
| Ā PTFE stirring blades, stainless steel rod with PTFE liner |
1 pc | |
| Ā Insulated hose with drain port & open/close valve x 2 Ā 3/8" Stainless steel hose barb adapters x 2 |
4 pcs |
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| Ā PTFE sealing tape | 1 pcĀ | |
| Ā PTFE stirring rod positioner/bearing kit |
1 set | |
| Ā Condenser dispenser connection kit | 1 set | |
| Ā Large opening material feeding port kit | 1 set | |
| Ā Bottom drain port sealing clamp | Ā 1 set | |
| Ā Rubber-wrapped condenser dispenser support and condenser bracket | 6 pcs | |
| Ā Chilling fluid connector x 2, vacuum connector x 1 |
3 sets | |
| Allen key (x 2) and backup inner hex set screws (5) and bolts (2) | 1 set | |
| Hose clamps | 5 pc | |
| SST Ball joint clamp | 2 pc | |
| Feeding funnel clamp | 1 pc | |
|
Motor Power Cord (110 or 220V) |
1 pc | |
| Motor Shaft Universal Joint | 1 pc | |
| NPT to barb fitting adapter | 2 pc | |
| #80 Quick Clamp | 1 pc | |
| #80 Centering Ring | 1 pc | |
|
Metal Support 28ā x1 Metal support 36ā with three boss heads x1 Metal support with five boss heads and one ring support |
3 pc | |
| Motor Support 29ā | 2 pc | |
| Ā User's manual | 1 pc |
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