Description
Ai R100 series jacketed glass reactors are designed for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Each reactor features adjustable stirring speeds and a constant pressure feeding funnel that allows you to add material to the vessel at a uniform and controlled speed. The built-in condenser makes it possible to recover some materials, also at a controlled rate of speed.
Features
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No more expensive heating circulators, no more messy heat transfer fluid, adapters and tubing. Introduing the new Ai ReactorHeater 200C heating jacket with temperature controller.
Ai 100L ReactorHeater with temp controller
- 200C maximum temperature
- 220V 50/60Hz 6,300 watts
- Speedy heating
- Ultra-thick insulation for minimum heat loss and very low outer jacket surface temperature
- Built-in open/close viewing window
- Easy installation, plug and play
- Oven-temp protection, over-current protection
- ETL tested to UL and CSA standards
- Designed and made in the USA
- ETL tested to UL and CSA standards (optional)
- Solvent-resistant PTFE on all sealing components ensures long time durability and operation.
- All glassware is hand-made from food grade high borosilicate glass that is heat/cold/corrosion-resistant.
- Adjustable stirring rate provides great torque or high speed.
- Patented PTFE stirring rod bearing for reliable and quiet operation.
- Optional multi-layer stirring blades for optimal reaction results.
- Large condenser cooling surface for exceptional condensation performance.
- Rugged stainless steel reinforced PTFE stirrer with anchored agitator, suitable for a wide range of viscous materials.
- Easily visual operation with digital speed and temperature displays.
- Heavy duty stainless steel supporting framework with lockable casters for mobility and stability. (whole support and glass vessel shipped pre-assembled)
- One year warranty and lifetime US-based parts, service, and support.
Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.
FAQ for Glass Reactor Series
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When do you recommend using the different impeller types that you have listed on the website?
The two different impeller types that we have is the pitched blade and the anchor agitator. It is recommended to use the pitched impeller for low viscosity solutions such as aqueous solutions and organic solvents. The anchor impeller is best used for higher viscosity applications such as thick oils, resins, and polymers.
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How do I clean my reactor?
The most effective and efficient way to clean your reactor would be by using the clean in place kit shown below paired with a pump capable of achieving between 10-20 psi.
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What is the best way to fill the reactor?
The best way to fill the reactor is to pull vacuum on the reactor from the condenser, and use either the stopcock on the lid or other fitting connected to a hose to pull the suck fluid into the reactor. As long as the other end of the tube is submerged in liquid and the pressure inside of the reactor is less than atmospheric pressure, fluid will enter the reactor.
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What are the materials of construction for the reactor’s wetted parts?
3 borosilicate glass and PTFE
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How long is the warranty period and what does it cover?
The length of the warranty is one year, and it covers manufacturing defects,
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What accessories come with the reactor?
The reactor will come with everything listed on the standard package for the unit that will be purchased. If purchasing an entire turnkey, please see the turnkey’s standard package. The standard package can be found on the web listing at Across International’s website under the standard package tab.
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Where can I find technical information about the Across International reactor?
Technical information can be found on the Across International website under the specifications tab. If further technical information is needed, please reach out to the sales team via email or phone at Across International: or 888-980899.
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What are the lid port sizes for my glass reactor?
The lid port sizes will vary depending on reactor type. Any port not labelled on the drawing is specific to Across International, take note that the QC-35 is also specific to Across International but clamps and adapters can be bought from Across International as needed for all lid adapters.
Lid for 10-50L reactor：
Lid for 100L-200L reactor:
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Will these sizes fit standard American ground glass joints? If so which ones will fit?
Please see the table below for a detailed description of which Across International glass reactor joints will fit the standard American ground glass joints:
|
Across International Joints Conical Joints |
Compatible American Standard Conical Joints |
|
40/38 |
40/50 |
|
34/35 |
34/45 |
|
24/29 |
24/40 |
|
14/23 |
14/35 |
| Model | R10 | R20 | R50 | R100 |
| Reactor power | 110V or 220V, 50/60Hz, 90W | 110V or 220V, 50/60Hz, 140W | 110V or 220V, 50/60Hz, 250W | |
| 200C heated jacket power |
220V 50/60Hz 2000W |
220V 50/60Hz 2100W | 220V 50/60Hz 3500W |
220V 50/60Hz 6300W |
| Reaction glass vessel capacity |
2.6 gallons (10L) | 5.3 gallons (20L) | 13 gallons (50L) | 26 gallons (100L) |
| Glass material | High borosilicate glass 3.3 | |||
| Rotation controller | Digital controller with variable frequency drive Rotation speed: 50 to 500 rpm |
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| Maximum jacket pressure |
4.4 psi or 0.03 MPa |
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| Drain valve | Flush seal design with large opening and flat flange clamp | |||
| Agitator | Style: impeller Material: 304 stainless steel with PTFE liner |
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| Funnel | Pressure equalizing | |||
| Vacuum gauge | Mechanical | |||
| Swivel caster | Four | |||
| Glass vessel temperature range |
-110F to 400F |
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| Vacuum level | 20 torr | |||
| Vacuum sealing | Glass or PTFE | |||
| Drain port ground clearance |
15 inches | 13 inches | 12.5 inches | 13.5 inches |
| Unit dimesions (WxDxH) | 18 x 26 x 78" |
20 x 27 x 80" |
26 x 33 x 85" |
28 x 42 x 95" |
| Shipping dimensions | 24 x 67 x 26" | 24 x 75 x 31" | 25 x 83 x 42" | 26 x 88 x 45" |
| Shipping weight | 240 Lbs | 262 Lbs | 330 Lbs | 460 Lbs |
| Compliance | ETL listed to UL and CSA standards (optional), CE (optional) | |||
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Part description |
Quantity |
Part image |
| Glass vessel, lid (7 Ports), clamps and heavy-duty stainless-steel stand with casters (shipped pre-assembled) |
1 set |
|
| Rubber bumper (pre-assembled) | 1 pc | |
| Lid gaskets (pre-assembled) | 1 set | |
| Upper and lower clamp set (pre-assembled) | 1 set | |
| Ai 200°C 100L heating jacket with PID controller and m 220V with 10-50P plug and mounting bracket | 1 pc | |
|
Vertical condenser with dual cooling coils, 2 chilling fluid ports, and 1 vacuum port, glass |
1 pc |
|
| Glass condenser dispenser with drain port and PTFE open/close valve |
1 set |
|
| Glass feeding funnel with PTFE open/close valve |
1 set | |
| Glass receiving flask with PTFE open/close valve | 1 set | |
| 1" Glass bottom drain port with PTFE open/close valve |
1 set |
|
| Glass vacuum valve (R-GVV34 x 2, R-GVV40 x 1, R-GVV24 x 3) |
6 pcs | |
| Stirring motor controller with material temperature display |
1 pc | |
| Stirring motor and motor support |
1 set | |
| Mechanical vacuum gauge with two 3/8" hose barb ports |
1 pc | |
| Temperature probe with PTFE seal |
1 pc | |
| PTFE stirring blades (3 blades), stainless steel rod with PTFE liner |
1 pc | |
| Insulated hose with drain port & open/close valve x 2 3/8" Stainless steel hose barb adapters x 2 |
4 pcs |
|
| PTFE sealing tape | 1 pc | |
| PTFE stirring rod positioner/bearing kit |
1 set | |
| Condenser dispenser connection kit | 1 set | |
| Large opening material feeding port kit | 1 set | |
| Bottom drain port sealing flange | 1 set | |
| Rubber-wrapped condenser dispenser support and condenser bracket | 5 pcs | |
| Chilling fluid connector x 2, vacuum connector x 1 |
3 sets | |
| Allen key (x 3) and backup inner hex set screws (6) and bolts (2) | 1 set | |
| Hose Clamps | 5 pcs | |
| Motor support rod | 1 pc | |
| SST ball joint clamp | 1 pc | |
| Feeding funnel clamp | 1 pc | |
| Motor Power Cord (110V or 220V) | 1 pc | |
| Motor Shaft Universal Joint | 1 pc | |
| User's manual | 1 pc |
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